Preparation of chinese herbal composite recipe used in horticulture

ABSTRACT

A recipe of Chinese herbal composite used in horticulture to kill pests. The practical applications of this recipe include pest killing, germ and virus eradication of vegetables, fruit trees, flowers and economical plants. This recipe is composed of  Gleditisia Sinensis, Sophora flavescens, Aloe uere, Stemona tuberose, Brucea jauamica  and  Dioscorea collettis  vice versa. We prepare it with modern principles and scientific methods to emulsion spray. Those so called modern and scientific are the emulsion processes, micronization, permeability and the multiply potency it possessed. Several laboratory and field test proved that this invention had definite effect on the past killing, germ eradiation and virus inhibition. This invention is belongs to non toxic Chinese herbal preparation. The spray does not harm or cause toxic effect as it touch human skin, eyes, nasal mucosa, lip, mouth and tongue. It does not accumulate in human body and pollute environment.

BACKGROUND OF THE INVENTION

1. Field of the Invention

The present invention relates generally to medicine, and more particularly to a Chinese herbal composite recipe and its preparation which used in horticulture to kill pests.

2. Description of the Related Art

The progress in material civilization in these 2 or 3 centuries bring many positive values to human beings. At the same time, there are many severe negative effects appear in ecosystem and environment. The population of the world increased and the horticulture and agriculture plants which feed human must increasing production. Therefore, under the negative changes and effects of the ecosystem, such crops must face the disturbance of disease, toxicity and pest and made it to produce difficultly.

The chemical agricultural chemicals propagate, because it's definitely killing effects and easily usage. It becomes the standby of production in farmers and always the most popular in the market. Until the mid of the twentieth centuries, the techniques of test and examination propagate. The senses of environment and pollution arose and proved gradually that such chemical toxins will remain toxin and pollution. They endanger human health and natural environment. The developed countries prohibit their production domestically. From Jan. 1, 2004, the European Allies will stop selling 320 kind of agricultural chemicals officially and import agricultural side products which polluted by such residues. In fact, the entrepreneurs knew that trend early and devote themselves in production and selling of low toxicity agricultural chemicals. They spent many capitals in research and development and the real effects of such low toxic products are far from those and make the resistance of virus and pest easily.

There are many records about agricultural pest killing, germ eradiation and toxin inhibition in the Chinese medical books. The pest killing plants, such as the Buddleia officinalis, Veratrum mentzeanum, Skimmia japonica, Euphorbia fischeriana steud, Sapindus mukorossii Gaertn, tobacco, Pyrethrum cineraefolium, Chalcanthite, Stemona tuberose, Gleditsia sinensis, Melia azedarach and vice versa. Therefore, the potent Chinese herbs do not according to the specifications of environment protection and sanitation. By the actual experiments, we can kill pests by 6:1 preparations if we can use non toxic Chinese herbs. It shows the conditional situations in economic benefits and usage applications. Therefore, we need some breakthrough in the idea to develop non toxic agricultural chemicals in Chinese herbs.

SUMMARY OF THE INVENTION

The objective of this invention is to provide a Chinese herbal composite recipe used in horticulture plants to kill pests, eradiate germs and in inhibit viruses. The modern and scientific extraction and preparation methods will augment 6 times and more than it's original potency. It will open the new applications and values of Chinese medicine. I hope it can replace synthetic agricultural chemicals and maintain agriculture profit, human health and avoid environment pollution and poisoning.

To achieve the objectives mentioned above of this invention, I supply the transformation mechanism, drug dispensing, drug preparation method, pharmacology description, range and method of application, caution, transformation and interior experiments and preliminarily field experiments.

DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS

The transformation mechanism called in this invention is the mechanism which to achieve more potency. It includes the theories used in traditional Chinese medicine, emulsion and permeability and micronization processes and vice versa.

Under the idea of avoiding poisonous Chinese herbs, the potency of organic Chinese herbs is hard to compete with the synthetic agricultural chemicals and pure chemicals.

However, it's principle of application is different to that of the synthetic agricultural chemicals and pure chemicals. It is not based on poison killing principle but on the theories of traditional Chinese medicine not to harm the body to eradiate germs or killing Ascarid, tape worm, hook worm, Nematode and inhibit poisons to heal the disease.

To increase potency on the original statement, the inventor analyzed the effective components of these drugs especially. To make them have multiply effects in assemble and preparation. I take reasonable concentration extraction to avoid the losses of alkaloids and necessary ingredients. Especially, I take more advanced and scientific grinding and colloid milling machine than original preparation method to perform micronized and special emulsion process.

The effects of pesticide, germicide and toxin inhibition of Chinese herbs is to promote drug entered from the derma and mucosa into the bodies of warms, this is the first step. This will cause the environment inside the body and the tissues change dramatically. To achieve such goals, the most important thing is the micronization of drugs and it's permeability except the composition of drugs and it does multiply effects. Therefore, this preparation uses some emulsion process to make water soluble emulsion because of the water soluble emulsion is easily absorbed by skin and mucosa.

The tension between liquid and gas is called surface tension. The liquids which do not intermingle each other, like the Molsa chinensis oil used in this preparation (the main ingredients are thymol, carvacreol and p-cymene), turpentine oil and the tension between the percolate is called the surface tension. The emulsified agents like yellow gelatin, Tragacantha, gum Arabic are belonging to surface active agents. They can reduce the surface tension between oil and percolate and down to 10 dyne/cm. The objective of emulsion is to make the oily effective ingredients into small droplets by emulsion agents and colloidal mill which supply energy from the outside world. That will make it micronized and more easily penetrate into worm bodies and to increase the absorption rate by derma and mucosa of worms and germs. That will change the interior environ of germs and worms dramatically.

As mentioned above, this is the mechanism of drug achieve effect and multiply potency. To prove this point of mechanism, the inventor performs the interior pest killing experiments (see interior experiment I) of transformation mechanism. That proved the turnover effect with emulsion added.

The Chinese compose recipe spray used in horticulture is prepared by Chinese herbs listed below, then I concentrated extraction and make powder by ratio with some definitely ratio percolate. Then I pulverized it by grinding and sieving with emulsified agents added.

(1) Concentrated Chinese powder and ratio.

-   -   Gleditsia sinensis 80˜120 gm Stemona tuberose 80˜120 gm     -   Sophora flavescens 80˜120 gm Brucea jauamica 80˜120 gm     -   Aloe uere 80˜120 gm

(2) Percolate and ratio.

-   -   distilled water 600˜800 ml alcohol 150˜250 ml     -   glycerin 80˜120 ml

(3) Emulsified agents used in original 3000 ml of solution.

-   -   Yellow gelatin or Gum arabic 40˜60 gm.     -   Turpentine oil 40˜60 ml.     -   Distilled Molsa chinensis oil 30˜50 ml.         Preparation

(1) Take concentrated Chinese composite recipe 1000 gm then passed milling machine for 2 to 3 times and soak for 2 hours. The first time percolate is 1200 ml. The second percolate is 1000 ml after soaking for 2 hours. Add distilled water 1200 ml and soak for 4 hours then percolate to get the third percolate. Combine these three percolates for later use.

(2) Take yellow gelatin or gum Arabic 50 gm and mix turpentine oil and Molsa chinensis oil 50 ml, respectively. Put them into colloid mill for high speed grinding than add distilled water 100 ml. Continue grinding for 3 to 5 minutes and repeat for 3 times.

(3) Adding 50 gm of Mirabilite and 3 gm of benzoic acid. Mixing them with (1) and (2). Passing them in golden mill and grinding 2 to 3 times.

Pharmacology

1. Gleditsia sinensis: Pesticide, germicide, toxin inhibition; contain gledinin and alkanes. It will increase permeability with other drugs.

2. Sophora flavescens: It has broad spectrum germicide effect and can help other drugs to kill pests.

3. Aloe uere: Pesticide, germicide, the lauric acid and myristic acid is helpful for mirabilite to promote solution penetration.

4. Stemona tuberose: Anti-microbe, pesticide, killing flied and mosquito and other 10 or more agricultural pests.

5. Brucea jauamica: Pesticide. The effect is enhanced by the gledinin and sodium sulfate (Mirabilite).

6. Dioscorea collettic: Germicide and pesticide. The important ingredient is saponin unit.

7. Molsa chinensis: It is extracted with distilled method. It contains pesticide and germicidal effects of essential oils like carvacrol, thymol and p-cymene. They make this preparation more delicate. I use it as the emulsion oil and make micronized material accomplish the assumed effect.

8. Turpentine oil: Germ resistance, germicide; emulsion oil.

9. Yellow gelatin: Emulsifying agent, protect plants.

10. Mirabilite: Working with other drugs to produce help and multiply effects to increase permeability and achieve pest and bacteria killing effects. (Please see drug description sheet for detail information.)

Range and Method of Application

1. This spray is applicable to economic crops, fruit trees, flowers, vegetables Lima bean. It also applies to general agricultural damages caused by pests, germs and viruses on crops.

2. Take this spray and dilute to certain ratios of water then spray on stems and leaves of crops or pests by manual or mechanical sprayer.

3. Depend on the order and families of pests, germs and viruses and the severity to determinate the dilution ratio.

Dilute 15 to 30 times for every pests, germs and toxins.

Dilute 30 to 60 times need 24 to 48 hours to kill or repel them.

Dilute 60 to 150 times has prevention effect.

4. The preparation is a contact pesticide. It shows eradiation effect on larva, adult and eggs. These pest and diseases can not produce resistance to this preparation. It do not block environ biological chains. You do not have to increase dilution ratio gradually. The prevention period can be extended. It is harmless to animals and human.

Caution

1. This invention is a topically Chinese medicine pest and germ killing agent. It is prohibited to take orally. It may cause gastrointestinal symptoms when take orally. You can purchase rare green bean powder, rare glycyrrhizin powder and talcum powder 6 gm, respectively. Mixing 6 gm of cold water with these things and take it. It will show some laxative effect or you should consult medical assistance.

2. The diluents of this preparation are harmless to animals and human. It do not cause any harm as contact with skin, eyes, nose, mouth and tongue.

3. This preparation should store in cool and dry places to prevent deterioration caused by high temperature.

Addendum

1. This horticultural Chinese composite spray is a quantitized concentrated Chinese extract powder. It is prepared by certain ingredients and ratio of percolate then dissolved in special emulsified agents.

2. This invention is the best practice of the Chinese composite recipe shown above. It can produce sufficient effect without adding Aloe. On the other side, the extraction of this recipe all using Dioscorea collettic powder as adjuvant but other drugs will do, too.

3. The feature of this preparation's re-extraction percolate is composed of the following ration of liquids.

4. Distilled water 60˜80%, alcohol 15˜25% and glycerin 8˜12%.

5. The feature of this preparation is the emulsion process. It adds yellow gelatin or gum Arabic with turpentine oil. Especially, I add essential oils of Chinese herb mainly thymol, carvacrol and p-cymene but others will do, too.

6. The other feature of this invention is adding 30 to 120 gm of Mirabilite (sodium sulfate) in to 3000 ml of original solution.

7. The feature of this preparation retains the right as application of environmental sanitation. That is to say, this invention and feature of preparation can be sprayed on the living environment to keep the sanitation of environ.

Drug Description Datasheet NO: 1 Name Zaolia Official name Gleditsia sinensis Dependence China Pharmacopoeia Volume IV pp 480 (China Sheng-Ghai scientific technology publication) Growing district, Grow in northeast, north collect season, south of China and Si-chuan, parts Qui-zhou province. Collect fruits and dry as they ripen and darken in autumn. Preparation, (1) Take 12 kg of Gleditsia extraction process, sinensis and soak in water for 6 method hours. Collect percolate for 2 times then evaporate the residue water to get 5 liters of fluid extract. Adding 2 kg Dioscorea collettii of powder and stir well. Drying it in 45° C. then pulverized by passing #120 sieve to make fine powder. Collect and store them for later use. Effective The capsules contain tri-terpene ingredient saponin that is gledinin saponin. Its basic saponin unit is gledinin, gledinin saponin, wax alcohol, novacosane, nor- septacosane, stigmasterol, sitosterol and tannin. Original recorded Germicide effect. The Gleditsia pharmacological sinensis extract show fungus effects inhibition effect on T. violaceum and Norcardis asteroids in skin. Fructus Gleditsiae abnormalis can kill larva of nematode and show hemolysis in vitro. The main feature is local mucosa stimulation effect. In central system, it can cause them convulsion and paralysis then death with breathe exhaustion. Pharmacological Pesticide and germicide ob- applications, jectives are achieved by the purposes ingredients contain in the Gleditsia sinensis such as saponins, alkanes and alcohols. They can cooperate with other drugs to promote penetration effect.

NO: 2 Name Kushen Official name Sophora flavescens Ait Dependence China Pharmacopoeia Volume IV pp 634 (China Sheng-Ghai scientific technology publication) Growing district, Grow in everywhere in China. collect season, Take all plants in September to parts October and remove the upper part, base of stem and fibrous roots. Cut fibrous roots into single strand. Wash out dirt then dry or bake it. Preparation, Take 12 kg of Sophora flavescens extraction process, and soak in water for 3 method hours. Collect percolate for 2 times then evaporate the residue water to get 5 liters of fluid extract. Adding 2 kg Dioscorea collettii of powder and stir well. Drying it in 60° C. then pulverized by passing #120 sieve to make fine powder. Collect and store them for later use. Effective The roots contain 13 alkaloids ingredient including matrine and many flavonoids mixtures. Otherwise, the roots contain tri-terpene saponin, soy saponin and kurarinone. Original recorded The in vitro experiments show pharmacological that 1% matrine has apparent effects bacteria inhibition effects on Shigella, E. Coli, Proteus, B-streptococcus and Staphylococcus aureaus. The total flavones of Sophora flavescens and their ethanol extract have killing or growth inhibition effects on Giardia lamblia Stiles in vitro. Pharmacological It can use specific alkaloids applications, and saponins to achieve goals of purposes killing pests and bacteria. The inventor observed 20 concentrated Chinese medicine drugs powder all using starch as adjuvant for 20 years and found that the Sophora flavescens did not eat into by worms and not change its quality. The package still remains intact. It shows the effect of germicide.

NO: 3 Name Luhui Official name Aloe uere L. var chinensis Dependence China Pharmacopoeia Volume VIII pp 51 (China Sheng-Ghai scientific technology publication) Growing district, Grow in Fu-jiann, Taiwan, collect season, Kuang-tong, Si-chuan, Yun-nan. parts Gather the middle and lower parts of leaves by batches separately. Cut the leaves open and collect liquids then drying it. The other way is to cut it and add the same part of water then boiling for 2 to 3 hours. Filtering, concentrating and drying. Preparation, Purchase pure and clean Aloe extraction process, concentrate blocks in the method market. Pulverized before use. Effective The leaves contain 11 acids ingredient such as Alesin, Aloe tannin, lauric acid, myristic acid and vice versa. There are some polysaccharides and sugar polymers. Original recorded Pesticide, germicide. pharmacological effects Pharmacological Lauric acid and the sodium applications, sulfate in the Mirabilite can purposes cooperative together to in- crease penetration ability into worm body.

NO: 4 Name Baibu Official name Stemona tuberose Lour Dependence China Pharmacopoeia Volume VIII pp 189 (China Sheng-Ghai scientific technology publication) Growing district, Stemona tuberose grows in collect season, southeast province of China, parts Hu-nan, Hu-peh and Si-chuan. Collect them after 3 years of planting. Remove tubers after wilting of upper parts of shoot before spring. Remove fine roots and boiling in hot water to well done then drying or baking them. Preparation, Take 12 kg of Sophora flavescens extraction process, and soak in water for 3 method hours. Collect percolate for 2 times then evaporate the residue water to get 5 liters of fluid extract. Adding 2 kg Dioscorea collettii of powder and stir well. Drying it in 60° C. then pulverized by passing #120 sieve to make fine powder. Collect and store them for later use. Effective The Stemona tuberose contains ingredient 13 alkaloids including syemonine, tuberostemonine and isotuberostemonine. It also contains sugar, fats, proteins, ash and 6 different acids including oxalic acid. Original recorded 1. Anti-microbe. pharmacological 2. Anti-parasite: In vitro tests effects show that 50% solution can kill pin worm in 20 hours. The tuberostemonine can paralyze Ascarid. 3. Insect killing effects: The Stemona tuberose water solution and alcohol solution has effects on lice and cause eggs of lice not hatch. It also show contact killing effect on 10 or more pests including maggot, larva of mosquito, bed bug, aphids, larva of Chilo simples and spider. Pharmacological Pesticide, germicide and anti- applications, viral effects. purposes

NO: 5 Name Yadanzi Official name Brucea jananica Dependence China Pharmacopoeia Volume V pp7 (China Sheng-Ghai scientific technology publication) Growing district, Grow mainly in Fu-kien, collect season, Taiwan, Hai-nan, Kwang-dong, parts Kwang-si, Yun-nan and Kwei- chow. The fruits ripen in autumn. Collect fruits as the skin of fruits darken then cleaning and drying. Preparation, Take 12 kg of Brucea jananica extraction process, and soak in water for 6 hours. method Collect percolate for 2 times then evaporate the residue water to get 5 liters of fluid extract. Adding 2 kg Dioscorea collettii of powder and stir well. Drying it in 45° C. then pulverized by passing #120 sieve to make fine powder. Collect and store them for later use. Effective It contains more than 30 in- ingredient gredients which structural similar to bitter ingredients of quassin. There are several glycosides including lignan of Hemerocallis fulva, vanillic acid and Hypericum. It also contains oleic acid, triglyceride and oil of Brucea jananica. Original recorded Anti-malaria and kill plas- pharmacological modium and amoeba. The crude effects extract can repel nematodes and tape worms in large intestine. It also has repelling effects on pin worm and Ascarid. Pharmacological It shows multiply effects with applications, Mirabilite and Gleditisia purposes sinensis and demonstrates the features pesticide effect.

NO: 6 Name Beixie Official name Discorea collettii Hook Dependence China Pharmacopoeia Volume VIII pp 231 (China Sheng-Ghai scientific technology publication) Growing district, Grow mainly in Che-kiang, Anh- collect season, wei, Jiang-si, Hu-nan. parts Digging the root stem in autumn and winter then remove the fibrous roots. Cleaning the dirt and slice for druying. Preparation, Take 10 kg of Discorea collettii extraction process, and pulverized by passing method #100 sieves to make fine powder as the adjuvant of collecting fluid extracts. Effective It contains 9 steroids. Dios - ingredient genin, Yamogenin, Δ 3,5-deoxy-tigogenin, Δ3,5- deoxy-neotigogenin, Diosgenin palmitate, Yamogenin palmitate, β-Sitoterol, a pair of Epimerides and two tzi-gan. Original recorded The water extract has insect pharmacological killing effects. It shows effective effects ingredients is discorea saponin. It has anti-fungal effect to Trichophyton and Giardia lamblia but no effect to bacteria. The Dioscorea collettii has the effect of fish poison but not apparently as tested. Pharmacological Pesticide and as adjuvant. applications, purposes

Drug Description Datasheet NO: 7 Name Howgining Official name Molsa chinensis Maxim. Dependence China Pharmacopoeia Volume VII pp 91 (China Shang-Ghai scientific technology publication) Growing district, It grows in east China, Taiwan, collect season, Kwei-chow. The flowers parts bloom in autumn and winter. Collect it as the stems and leaves prosper. Drying under shade and pack into small bundles. Preparation, Take 12 kg of Molsa chinensis extraction process, and chop into fine stripes. method Place them into distillation barrel and press firmly. Using heat to perform partial distillation in order to get the essential oil about 240 ml. Remove the remainder and store the essential oil in the bottle for later use. Effective The Molsa chinensis is called ingredient the Shi-xiang-ru. The total plant contains volatile oil 2% in- cluding carvacrol 71.64%, p-cymene 10.10%, p-isopropyl phenyl methyl alcohol 5%, β- pinene 1.52%, terpineol 1.23%, thymol 1.40%, caryophyllene 1.36%, β-farnesene 0.25%, limonene 0.15%. Original recorded The Molsa chinensis volatile pharmacological oil possesses stronger broad effects spectrum germicide effect. The main effective anti-bacterial ingredients are thymol, carvacrol and p-cymene. Pharmacological Used as emulsifying oil. It applications, can potentiate the pesticide, purposes germicide potency of essential oils and bring other pest and germ killing agents' potency.

NO: 8 Emulsifying oil Name Songlievou Official name Pinus oil Dependence China Pharmacopoeia Volume II pp 305 (China Shang-Ghai scientific technology publication) Growing district, It grows mainly in Kwang-dong collect season, and other provinces. We get parts the volatile oils distilled or extracted from the oily resin. Preparation, Purchase authentic pure and extraction process, clean turpentine for later use. method Effective It contains resin acids, fatty ingredient acids, mono-terpines and semi-terpines Original recorded 1. Anti-microbe effect. In pharmacological vitro experiments show stronger effects anti-fungal effects (Candida albicans) on Tinea corporis and dermatophytosis It has certain degree of germ inhibition effects on Staphylococcus aureaus and E. Coli. It is used ad emulsifying oil in this preparation. Pharmacological Emulsifying agent, germicide applications, and parasite repelling. purposes

NO: 9 Emulsifying agent Name Yellow gelatin Official Colla corii name Bon's Dependence China Pharmacopoeia Volume IX pp 680 (China Sheng-Ghai scientific technology publication) Growing district, Chop dried yellow ox leather collect season, into small cubes. Adding them parts into water and soak for 2 days. You must change water and stirring well frequently. Cleaning it as the leather soften and put into copper pot. Boiling it gently with 5 times of water. Adding water frequently and filtering supernatant for every 24 hours. Repeat these for 3 times. Precipitate the supernatant with alunite and pour the super- natant. Re-heat and condense in the copper pot till the liquid do not absorb by filtering paper. Adding some yellow wine or candy sugar to collect the gelatin. Pour it into the plate and cool. Chop it into small pieces for drying. Preparation, Take pure clear yellow gelatin extraction process, from market and pulverized method into powder. Effective Collagen in the leather of the ingredient yellow ox is not soluble in water. Boiling with water for a long period can transform collagen into water soluble yellow gelatin. It contains nitrogen, sugar, multiple vitamins and helpful to plant growth. Original recorded pharmacological effects Pharmacological Promote growth of plants. It is applications, used as emulsifying agent in purposes this invention.

NO: 10 Agumenter Name Puxiao Official name Mirabilite Dependence China Pharmacopoeia Volume I pp 269 (China Shang-Ghai scientific technology publication) Growing district, collect season, parts Preparation, Purchase authentic Mirabilite extraction process, for later use. method Effective Hydrated sodium sulfate ingredient (Na2SO4-10H2O) mainly with trace sodium chloride and in- organic elements such as calcium, magnesium and potassium. Use it to penetrate and soften. Original recorded pharmacological effects Pharmacological To produce cooperative or applications, additional effect with drugs such purposes as Aloe uere, Gleditsia sinensis, Brucea jauamica and vice versa. It can promote pesticide, germicide and penetration effects.

Field experiment example I Notolophus Australia posticus, Chlorita flavescens and tea red spider in tea tree farm. Objective of experiment The effect of this invention is applied to the pest in the tree farm. Time and place Apr. 13, 2003. #1123 in Xin-kai Section, Liu-gui, Kaohsiung county. Environment There are 20 acres of dry land with elevation of 800 meters. Tea trees grow in 1983 then betel trees in 1990. Status of 1. Many diverse of tea trees pest damage and back of old leaves found larva of red spiders and some old leaves fallen. 2. The fresh leaves have bite wounds. Shaking the bush and found Chlorita flavescens flying everywhere. The situation is getting worse. 3. The down-left area of this tea tree farm appear larva of Notolophus Australia posticus. Pest name 1. Tea red spider is called and brief tea mite. It's very tiny. The description female is ellipse shaped and length is 0.34 mm. The male one is small shield shaped. The color is purple-red or deep red. The color in the back is faint. There are loose white fine hairs in the body. The legs are pale-red color. The larvas have 3 pairs of les and the adult has 4 pairs of legs. They damage old tea tree leaves and make them wither and fall. 2. Chlorita flavescens is called tea cicada. It is fragile. The body length is 1 to 3 mm with pale green and transparent body. The fore- wing is yellow only. They suck the juice of fresh leaves and block the development of tea tree leaves. The damages leaves are shrinking with faint-yellow color and the rim of leaves become brown. The leaves scroll into ship shape and fallen. 3. Notolophus Australia posticus is called red-head poison caterpillar or stinky dog. The body length is 22 to 30 mm. The body color is variable depend on seasons. In summer, the head is red and the body is in light yellow. There are may yellow and white long hairs all over the worm body. It will cause allergic itch and pain as touched human skin. They eat leaves of tea trees and damage severely in March to May. General Use 100 times of water with status of 1 part of this preparation. application Apply it with mobile sprayer. There are about 2000 tea trees. The original solution of this preparation used is 3 liters and 157 liters of water. Effect Inspect at afternoon of Apr. evaluation 14, 2004. There are no tea mites found and no Chlorita flavescens flying as shaking bushes. The Notolophus Australia posticus died in the ground. Inspect at afternoon of Apr. 20, 2004. The shoots of tea trees grow normally and no pests seen. postscript Actually, from the beginning of this tea tree farm opened. I always using Chinese medicine powder to dilute 150 times and proved effective. Now, I improved it into emulsion and dilute into 100 times and the effect more apparently.

Field experiment example II Pesudaulacaspis pentagonai in magnolia tree. Objective of The effects of this invention experiment apply to the Pesudaulacaspis pentagonai in magnolia tree. Time and Nov. 24, 2003. #1123 in place Xin-kai Section, Liu-qui, Kaohsiung county. Environment The magnolia tree is 20 years old and grew in front of the house. Status of There are 2 magnolia trees pest damage in these experiments. They have damaged by Pesudaulacaspis pentagonai for many years. The middle sections of the stem always show gray-white appearance. This appearance may extend to the twig and make the upper part green leaves of the damaged section withering. The blooms are weak and small. The twigs died at last. The trees is so big and good drainage and fresh air make them live till today. I can fell the humidity of larva and odor as touch the surface of the stem with hands. Pest name Pesudaulacaspis pentagonai and brief Targioni-Tozzett is hosted on description Melia azedarach, prune, plum, peach, almond tree, apple tree, magnolia tree and Hibiiscus mutabilis. The worms attach itself on the base of the stems first. The damages skin form gray-white or powder like sign. The larva and female suck juice and extend to the tip of twigs. The damaged twigs withering, drying and falling. The male is 0.75 mm in length with red color and its head is brown. It possesses antennas. The pro- boscis is degenerate and a pair of transparent wings on it. The legs are slender and the coupler is in needle shape. The female adult one is 1.3 mm in length. The body is hidden under the flat or slightly round gray-white shell with pale red-orange color. She has no antennas and wings. The proboscis is very sophisticated. The shell is round or short ellipse in white of gray-white color. The center has an umbilical spot. The diameter is 1.8 to 2.5 mm. The larva is flat and elliptic with pale yellow color. They secret shell and live under it after one exuviate. Proboscis General Use 30 times of water with 1 status of part of this preparation. application Apply it with mobile sprayer evenly on the gray-white twigs till all twigs are wetted. Effect I fell the stem damaged by evaluation pests were dry after 7 days of application. There are no pests and odor. After 14 days, The gray-white shells fall- ing gradually. The upper part leaves of pest damaged are turning green. postscript

Field experiment example III Aphids in Solanum nigrum. Objective of The effect of this invention experiment is applied to the Aphids in Solanum nigrum. Time and Nov. 17, 2003. #1123 in place Xin-kai Section, Liu-qui, Kaohsiung county. Environment Left part of the house grows Eapatorium fortunei, Eapatorium Chinese and Solanum nigrum. Status of The Solanum nigrum are about pest damage 30. The twigs and leaves have transparent Aphids stay on it. The leaves curled and development retarded. Pest name Aphids have many species. and brief They all belong to Order description homoptera, Family Aphididae. The body length smaller than 3 mm. they always gather together to feed on leaved and fresh shoots or hide under recesses of fruits. The damage by group suction. The Aphids excrete honey droplets and we can see ants and coal dip as plants damaged by Aphids. That is the general identification knowledge of Aphids damage. General Use 30 times of water with status of 1 part of this preparation. application Apply it with mobile sprayer on all twigs. Effect Inspect in Nov 23, 2003. evaluation There are no trace of Aphids on the stems and leaves of Solanum nigrum. The curled leaves show some extend. There are coal dips on the leaves but no Aphids seen. postscript The inventor practice Chinese medicine in Gang-shan town as a physician. He will back to Liu-qui by afternoon Sunday regularly and back to Gang-shan at Monday. The evaluation must performed at Nov 23 because of the Nov 17 is Monday by himself.

Field Experiment Example IV Ring Spot Virus Disease Objective of The effect of this invention experiment is applied to the sick plants infected by ring spot virus. Time and Nov. 02, 2003. #1123 in place Xin-kai Section, Liu-qui, Kaohsiung county. Environment In front of the house. Status The original developed normally of pest Papaya trees had bloomed in damage August and September. In October, its inner leaves (Newly grow top leaves) appeared dotted line yellow spots. The yellowish shrink and the veins of leaves shown green stripes with apparent etched stripes. The development is retarded. Pest name Ring spot virus of Papaya tree is and brief belonging to virus disease. It is description different from pest and germ damages. It is appeared first time in Yan-cao, Kaohsiung county in 1975 and spread all over the province in 1 to 2 years. It is called “wild plant”. It is spread by winged Aphids and machine recorded by agricultural experts. The features of this disease are the center leaves become yellow and shrink. The veins of leave are striped with vivid etched stripes. The sick leaves are smaller than normal leaves. The rim of leaves dried gradually and leaves fall. Only top survive or fall totally and cause death. The sick plants appear oil soaked spots or stripes in petioles and stems. The plants have small short petioles. There are oil soaked spots and stripes on the petals. Usually bloom but do not fruit. The fruits appear round or elliptic ring stripes. The sick plant can fruit continuously and the sick fruits lose value of merchandise or usage of application. General status Use 30 times of water with 1 of application part of this preparation. Apply it with mobile sprayer on all twigs. Effect Seven days after spray, There evaluation are no apparent differences between these 2 areas. After 14 days, The sick leaves shown brown spots. After 30 days, The new grow central leaves of south area appear striped yellow spots and the leaves look weak and wither. The central leaves of north area appear normal green color and the leaves look strong and prosper. The lower layer of developing leaves appear normal but the control group is withering and yellow. postscript The ring spot virus disease in Taiwan has been propagated for near 30 years. There is no effective drugs appear. They have no choice to use net house to culture them. The loss of annual agriculture is very huge. This appear of this invention is vividly a great Evangel. It needs to spray 3 to 4 times per year.

Field experiment example V prevention of lima bean fruit fly. Objective of The effect of this invention experiment is applied to the lima bean fruit fly. Time and place Nov. 09, 2003. #1123 in Xin-kai Section, Liu-qui, Kaohsiung county Environment Tented net style. The area is about 7 square meters. I plant 2 lima beans and fertile and irri- gation as usual. The leaves and stems have spread on the net all. It is the period of bloom and fruiting. Status of The fresh bean capsule pest damage appear soften and falling phenomenon. There are bite trace near the head of the fresh buds. Yellow- white larva in the capsules after ripping the outer skin. The beans have the bite appearance. Some insects loitering and flying during white flower of bean bloom. Pest name The adult is larger and brief than oriental fruit fly. description By consulting the agricultural pest control data, identi- fied as Daus cucrbitae Coeuilltt. It is belong to order Diptera, family Tephritidae. The main host plants are melon or tomato and Legurninosae. The color of the adult is yellow-brown. Body length is 8 to 14 mm with red-yellow legs and big wings. It looks like bee or fly. The purpose of this fly jumping between flowers is to increase its reproductive ability. It place eggs Insert into fruits. The larva hatched and feed in the fruits. The damaged fruits change shapes, falling or stop growing. The larva falls to the ground and make cocoon to reproduce. General status Use 30 times of water of application with 1 part of this preparation. Apply it with mobile sprayer on all stems and leaves and wetted them all then spray on the ground. Effect Some fruit flies fly evaluation away during spray. Some of them dropped and loss of flying ability. And die after 2 to 4 hours. There are no fruit flies flying observed in Nov 16, 2003. Some survived lima beams can harvest. postscript Inspect in Nov. 25, 2003. There are some fruit flies appear again. You need to spray every 2 weeks and have to spray onto the ground to make the cocoons of fruit flies loss of opportunities for reproduction.

Field Experiment Example I (Comparison of Transformation) Objective of Comparison of pest killing experiment effects on preparation (1) no emulsion, (2) emulsion. Time and DEC. 14, 2003. #62 place Sho-hwa Road, Gang-shan, Kaohsiung county in laboratory. Pest sampling Taking larva of Piens rapae Cruciuora Boisdurol from cabbage of private experi- ment garden and larva of Hellula rogatalis from Cassia obtusifolia. They are healthy worms. Brief Piens rapae Cruciuora Boisdurol description is called green worm. of pest The larva with green head and fine hairs on the body. Body length is about 2.5 to 3 cm. They feed on leaves and leave cores. You can found large quantities of feces in the base of leaves in the damaged plants. Hellula rogatalis is called vegetable worm or bean worm. The larva is 2 to 2.5 cm in length with black-brown head. Its body is green with annular rings and three white longitudal line and thick gray line in both body sides. They feed on leaves until petioles left. There are feces and silk strings between leaves. Those who digging into the core leaves of Cruciferae plants or cabbages and feed on it are in third stage larva. Pre- Put test larva on filtering experiment papers to avoid soaking. Using small hand sprayer to spray 3 times from left to right, right to left and far to near, all focus as the worms as the center. Then move the worms and filtering papers in to glass cabin for observation. Experiment 1. This invention can be procedure divided into no emulsion (1) and emulsion (2). 2. Then dilute it into 6 parts such as 5:1, 10:1, 15:1, 20:1, 25:1 and 30:1, respectively. 3. Take 6 Hellula rogatalis and 4 Piens rapae Cruciuora Boisdurol to perform experiment. 4. Observe time for result is 2 minutes after spray and 180 minutes, respectively. Description and 1. Depend on pharmacology conclusion and many results recorded from experiments. They show in situ movement only or stop moving in 2 minutes and I can not make sure they are death. The reason could be the paralysis effects of drugs or drugs can not penetrate into worm bodies. It is possible for them to re-vital in 30 to 60 minutes. I must make sure that they stop moving after 2 hours and realize that they are dead. For prudently, I determine it after 3 hours. 2. The difference between (1) and (2) is on the emulsion. The ingredients and adjuvant are the same. 3. Under 5:1 dilution ratio, stop moving (in 2 minutes) in preparation 1 are count 10 and preparation 2 show in situ movement of secondary potency. This is because of preparation 2 has added emulsion and the solution is too thick. The drug content is enough so 180 minutes left there are no crawling worms. The in situ movement worms show fatigue and grad- ually go to death. 4. Observe the situation and changes under dilution 15:1 and 30:1, we can find that worms' number in situ movement and crawling in preparation 1 are increasing. The in situ movement one do not show fatigue and will re-vital again. On the contrary, 2 worms in the 30:1 after 180 minutes in preparation 2 are all dead. 5. From the list shown above. Emulsified Chinese medicine herbal pest and germ killing preparation can increase 6 times of potency indeed. 6. Prepared by emulsion can enhance the potency of Chinese medicine herbs and it is the important feature of this invention. It is a new invention.

Experiment list (Hellula rogatalis, Piens rapae Cruciuora Boisdurol) Worm (1)No emulsion (2)Emulsion Dilution body 1(in 2(after 180 1(in 2(after 180 ratio status 2 mins) mins) 2 mins) mins) 5:1 Stop 10 6 0 8 moving In situ 0 4 10 2 movement Crawling 0 0 0 0 10:1 Stop 5 3 4 10 moving In situ 5 7 6 0 movement Crawling 0 0 0 0 15:1 Stop 5 3 10 10 moving In situ 5 7 0 0 movement Crawling 0 0 0 0 20:1 Stop 0 2 10 10 moving In situ 10 8 0 0 movement Crawling 0 0 0 0 25:1 Stop 0 0 10 10 moving In situ 10 5 0 0 movement Crawling 0 5 0 0 30:1 Stop 0 0 8 10 moving In situ 10 3 2 0 movement Crawling 0 7 0 0 p.s.: Stop moving: There are 2 situations of paralysis fake death and death. Death means stop moving after 180 minutes. In situ movement: It means the worm do not move everywhere but still alive as touch it by probe. We need to observe it is fatigue or not after 180 minute in situ movement. The fatigue one will die. Crawling: It means the worm still has the ability to crawling.

Interior Experiment Example II (Eradiation of Plutella xylostella) Objective of The effect of killing experiment Plutella xylostella in diluted emulsified preparation. Time and Nov. 29, 2003. place #62 Sho-hwa Road, Gang-shan, Kaohsiung county in laboratory. Pest Pests were taken sampling from Chiang-chi, Ping-dung county by working staff from coleseed shoots in glass greenhouse. Brief Plutella xylostella description L. is called of pest silk-hanging worm. It is belong to order Lepidoptera, family Plutellidae. The larva all hosted in Cruciferae. It likes cabbage, Broccoli, Chinese radish and coleseed. The usual larva is in the third or fourth stage and body length is under 1.3 cm. The color is green or kahki with apparent segmentation. It will fall upon stirring. It use silk to connect leaves and hanging in the air and is called silk-hanging worm. The larva digging into leaves and feed on it then moving to back of leaves after the second stage and make leaves broken. When the plants are small, they always gather together in the central leaves and spit silk to protect them and make plants can not sprout and causing death. This worm can have 20 generations in a year and possess extraordinary reproductive ability. Pre- Put test larva on experiment filtering papers to avoid soaking. Using small hand sprayer to spray 3 times from left to right, right to left and far to near, all focus as the worms as the center. Then move the worms and filtering papers in to glass cabin for observation. Experiment 1. This preparation procedure is dilute into 15:1, 20:1, 25:1, 30:1, and 40:1, respectively. 2. Choose same size 10 Plutella xylostella for testing. Description The worms die and conclusion with head bending backward and shaking. Observe after 180 minutes and found the middle section of worm bodies show dark green or black. I can make sure that all worms are killed with dilu- tion ratio 15:1 to 30:1. There are 2 worms still have residue life in dilution ratio 40:1.

Experiment List of Plutella xylostella (Silk-hanging worm) Dilution 1(in 2(after ratio Worm body status 2 mins) 180 mins) 15:1 Stop moving 10 10 In situ 0 0 Crawling 0 0 20:1 Stop moving 10 10 In situ 0 0 Crawling 0 0 25:1 Stop moving 10 10 In situ 0 0 Crawling 0 0 30:1 Stop moving 8 10 In situ 1 0 Crawling 1 0 40:1 Stop moving 6 8 In situ 2 2 Crawling 2 0

Interior Experiment Example III (Eradiation of Oebia undalis) Objective of The effect of killing experiment Plutella xylostella in diluted emulsified preparation. Time and Dec. 07, 2003. place #1 Cha-shen Road, Liu-qui, Kaohsiung county. Pest sampling From farmer Mr. jia-mow, Ho. Brief Oebia undalis Fabriciu description S. is called of pest “vegetable worm”, “vegetable core worm”, “radish worm” and “core-drilling worm”. It is belong to order Lepidoptera, family Pyralidae. The larva damage radish severely in Taiwan. It also damages other plants of Cruciferae. It will dig into core leaves and feed on it and also turn into stems or over-ground roots. Drilling many hole in it. You can see many feces accumulated outside these pores. Ripping the damages parts and found larva about 0.8 cm in length with black head. There are 5 longitudal lines from foreside to the tail. The adult is about 1 cm in length. Pre- Put test worm on experiment wrapping papers and use small hand sprayer to spray 3 times from left to right, right to left and far to near. Let the table incline immediately to avoid soaking. Observe within 2 minutes and remove worms into ventilated plastic bottles and place some clean and fresh leaves. Experiment 1. This preparation procedure is dilute into 15:1, 20:1, 25:1, 30:1, and 40:1, respectively. 2. Choose same size 10 Plutella xylostella for testing. Description After 180 minutes, and conclusion there are still 1 to 2 worms can crawling with dilution 25:1 and 30:1. It is ob- vious that the Oebia undalis is more re- sistant than Piens rapae Cruciuora and Plutella xylostella.

Experiment List of Oebia undalis (Core-Drilling Worm) Dilution 1(in 2(after ratio Worm body status 2 mins) 180 mins) 10:1 Stop moving 10 10 In situ 0 0 Crawling 0 0 15:1 Stop moving 10 10 In situ 0 0 Crawling 0 0 25:1 Stop moving 8 9 In situ 2 1 Crawling 0 0 30:1 Stop moving 5 4 In situ 3 4 Crawling 2 2

Interior Experiment Example VI (Eradiation of Plutella xylostella and Piens rapae) Objective To test the prevention effect of this preparation and effect o of ex- growth of plants. periment Time and Plant in Oct. 27, 2003 in #0148-0048 Wan-tze-nei section, place Gang-shen town Ex- By normal plant methods, divide into A, B and C areas. periment Each area plant 20 cabbages. The area A is the experiment design area and Areas B and C are control. The fertilizing and irrigation are as the usual ways. Imple- Plant cabbage shoots in Oct. 27, 2003. mentation Nov 3 Spray area A in 30:1 dilution ratio with manual procedure sprayer. The controls do not spray. Nov 10 Area A does not show sign of worm damage and no eggs found. Today do not spray. The control areas found 6 Plutella xylostella and some eggs. Nov 17 Area A has 1 plant damaged by worm. One Piens rapae found. Spray with 30:1 solution. The control areas found 3 Piens rapae and 4 Plutella xylostella. Nov 24 Area A does not show sign of worm damage and no worms found. Today do not spray. The control areas found 2 Piens rapae and 6 Plutella xylostella. Dec 1 Area A does not show sign of worm damage. Spray with 50:1 solution. The control areas found 2 Piens rapae and 8 Plutella xylostella. Dec 8 Area A does not show sign of worm damage and no worms found. Today do not spray. The control areas found 3 Piens rapae and 6 Plutella xylostella. Dec 15 Area A does not show sign of worm damage. Spray with 60:1 solution. Today do not spray. The control areas found 2 Piens rapae and 4 Plutella xylostella. Dec 29 Area A does not show sign of worm damage and no worms found. The control areas found 6 Piens rapae and 4 Plutella xylostella. Effect 1. Spray area A every 14 days. I grab 1 green worm in Nov evaluation 17 and there are no damage till Dec. 29, 2003 2. The dilution ratio in spray gradually increased from 30 to 60:1 and the dosage decrease still effective. 3. The cabbage is ripped at Dec. 29, 2003. The growth status show no difference but the controls have 4 plants with bad formation. 

1. A Chinese medicine composite recipe used in horticulture for pesticide comprising at least Gleditsia sinensis, Sophora flavescens, Stemona tuberose, Brucea janamica, and Mirabilite, said Chinese medicine composite recipe being prepared by being dissolved in emulsifying agents.
 2. The Chinese medicine composite recipe as defined in claim 1, wherein said emulsifying agent comprising yellow gelatin or gum Arabic with terpentine and Chinese medicine essential oils essentially consisting of thymol, carvacrol, and p-cymene.
 3. The Chinese medicine composite recipe as defined in claim 2 further comprising Molsa chinensis, said Molsa chinensis having Chinese medicine essential oils essentially consisting of thymol, carvacrol, and p-cymene.
 4. The Chinese medicine composite recipe as defined in claim 3 further comprising Aloe uere.
 5. The Chinese medicine composite recipe as defined in claim 4 further comprising pesticidal Dioscorea collettic as adjuvant.
 6. A horticultural pesticidal agent in every 3000 ml of percolate in component proportion comprising Chinese medicine fine powders of Gleditsia sinensis 80-120 gm, Sophora flavescens 80-120 gm, Stemona tuberose 100-140 gm, Brucea janamica 100-140 gm and Mirabilite 30-120 gm, said Chinese medicine fine powder being dissolved in emulsifying agent.
 7. The horticultural pesticidal agent as defined in claim 6, wherein said percolate is prepared by liquids in component proportion comprising distilled water 60-80%, alcohol 15-25%, and glycerin 8-12%.
 8. The horticultural pesticidal agent as defined in claim 6 further comprising lign aloes 60-100 gm.
 9. The horticultural pesticidal agent as defined in claim 6, wherein said emulsifying agent comprises yellow gelatin or gum Arabic 40-60 gm, turpentine 40-60 ml, and distilled Molsa chinensis oil 30-50 ml.
 10. A manufacturing method for horticultural pesticide comprising steps of adding powders of Chinese medicine of Gleditsia sinensis, Sophora flavescens, Stemona tuberose, and Brucea jauamica into percolate for filtering process, proceeding with emulsifying process by emulsifying agent, adding Mirabilite for mixing.
 11. The manufacturing method as defined in claim 10, wherein said percolate of every 3000 ml in component proportion comprising Chinese medicine fine powders of Gleditsia sinensis 80-120 gm, Sophora flavescens 80-120 gm, Stemona tuberose 100-140 gm, Brucea jauamica 100-140 gm, and Mirabilite 30-120 gm.
 12. The manufacturing method as defined in claim 11, wherein said emulsifying agent used in said emulsifying process comprises yellow gelatin or gum Arabic 40-60 gm, turpentine 40-60 ml, and distilled Molsa chinensis oil 30-50 ml.
 13. The manufacturing method as defined in claim 11, wherein said filtering process comprising steps of the Chinese medicine fine powder being percolate for the first time to get 1200 ml of percolate, then being passed through milling machine for 2 to 3 times and soak for 2 hours then being filtered, the second percolate being 1000 ml and filtered after soaking for 2 hours, the third percolate being added 1200 ml of distilled water then soak for 4 hours then filtered, combining the three percolate for later use.
 14. The manufacturing method as defined in claim 11, wherein said emulsifying process comprising steps of respectively adding yellow gelatin or gum Arabic 50 gm with turpentine and Molsa chinensis oil 50 ml, pouring them into colloid mill for high speed milling, adding 100 ml of distilled water into it and milling for 3-5 minutes, repeating for 3 times, and adding filtrate from percolate and milling for 3 times.
 15. The manufacturing method as defined in claim 13, wherein said emulsifying process comprising steps of respectively adding yellow gelatin or gum Arabic 50 gm with turpentine and Molsa chinensis oil 50 ml, pouring them into colloid mill for high speed milling, adding 100 ml of distilled water into it and milling for 3-5 minutes, repeating for 3 times, and adding filtrate from percolate and milling for 3 times.
 16. The manufacturing method as defined in claim 11, wherein said Chinese medicine fine powders comprising Aloe uere 60-100 gm.
 17. The manufacturing method as defined in claim 15, wherein said Chinese medicine fine powders comprising Aloe uere 60-100 gm.
 18. The manufacturing method as defined in claim 11, wherein said mixing process of Mirabilite comprising steps of adding 50 gm of Mirabilite and 3 gm of benzoic acid with percolate after emulsifying process, mixing well, and passing them to the golden mill and milling 2 or 3 times.
 19. The manufacturing method as defined in claim 11, wherein said mixing process of Mirabilite comprising steps of adding 50 gm of Mirabilite and 3 gm of benzoic acid with percolate after emulsifying process and mixing well, and passing them to the golden mill and milling for 2 or 3 times.
 20. A Chinese medicine composite recipe for environmental sanitation omcrising at least Gleditsia sinensis, Sophora flavescens, Stemona tuberose, Brucea janamica, and Mirabilite, Chinese medicine composite recipe being prepared by being dissolved in emulsifying agent.
 21. The Chinese medicine composite recipe as defined in claim 20, wherein saod emulsifying agent comprises yellow gelatin or gum Arabi, turpentine, and Chinese medicine essential oils essentially consisting of thymol, carvacrol, and p-cymene.
 22. The Chinese medicine composite recipe as defined in claim 21 further comprising Molsa chinensis, said Molsa chinensis having Chinese medicine essential oils essentially consisting of thymol, carvacrol, and p-cymene.
 23. The Chinese medicine composite recipe as defined in claim 22 further comprising Aloe uere.
 24. The Chinese medicine composite recipe as defined in claim 22 further comprising pesticidal Dioscorea collettic as adjuvant. 